11.01.05
Deionized water | 51.587 |
Disodium EDTA (Versene NA2, Dow) | 0.051 |
Carbomer (Carbopol ultrez 10, Noveon) | 0.051 |
Butylene glycol (1,3 Butylene glycol, Celanese) | 4.038 |
Phenoxyethanol, methylparaben, ethylparaben, butylparaben, propylparaben, isobutylparaben (Co-Sept PEP, RTD HallStar) | 0.607 |
Triethanolamine (Trolamine 99 N.F., Ineos) | 1.967 |
Octisalate (HallBrite OS USP, RTD HallStar) | 5.085 |
Homosalate (HallBrite HS USP, RTD HallStar) | 7.627 |
Diethylhexyl 2,6-Naphthalate (Corapan TQ, Symrise) | 5.085 |
Dimethyl capramide (Spectrasolv DMDA, RTD HallStar) | 2.034 |
Adipic /NPG/ bis-Cyanodiphenyl-propenoate /octyldodecyladipate copolymer (Polycrylene, RTD HallStar) | 2.045 |
Avobenzone (Parsol 1789, DSM Nutritional) | 3.051 |
Oxybenzone (Neo Heliopan BB, Symrise) | 4.183 |
Polyglyceryl-3 distearate (Cremophor GS 32, BASF) | 3.205 |
Sorbitan Isostearate (Crill6, Croda) | 4.298 |
Stearic acid (RTD Stearic acid V-1655, RTD HallStar) | 3.255 |
C30-38 olefin/isopropyl maleate/MA copolymer (Performa V 1608, New Phase Technologies) | 0.812 |
Polyacrylamide, C13-14 isoparaffin, Laureth-7 (HallGel 305, RTD HallStar) | 1.019 |
Procedure | |
In the primary vessel dissolve 2 in 1 and then stop mixing and sprinkle on 3. When 3 has fully wetted, resume mixing. In a separate vessel combine 4, 5 and 6 and then add to main vessel and heat this water phase to 80°C. To the secondary vessel add 7,8,9 and 10 and start mixing and heating this oil phase to 85°C. Add 11, 12 and 13 when the oil phase is at 50°C. When the oil phase is at 85°C, add 14, 15, 16 and 17. When both phases are homogeneous and at their designated temperatures, add the oil phase to the water phase with continued mixing without aeration. Maintain heat, mixing for five minutes and then homogenize for one minute (until a fine white emulsion is formed). Stop homogenizing, resume mixing and start cooling. When the batch is below 45°C, add 18. Mix until the batch is creamy smooth and below 35°C and then replace any water lost to evaporation. When again uniform, stop cooling and mixing and perform final quality assurance checks. | |
More Information | |
RTD HallStar, 1500 Rt. 517, Suite 305, Hackettstown, NJ 07840-2717 Tel: (908) 852-6128; Fax: (908) 852-1335 E-mail: rtdhallstar@cphall.com; Website: www.rtdhallstar.com |