Formulary

Spider Web Créme Wax

March 1, 2009


Phase A
Deionized water
6.00
Propylene glycol
8.00
Polyox WSR-301 (Dow/Amerchol) (PEG-90M)
0.24
Cremophor A 25 (BASF Corp.) (Ceteareth-25)
5.00
Schercemol PDD Ester (Lubrizol Adv. Mat.) (Diisostearoyl polyglyceryl-3 dimer dilinoleate)
2.00
Petrolato Ambar 158 (Drogueria Cosmopolitan) (Petrolatum)
4.00
Dow Corning 556 Cosmetic Grade Fluid (Dow Corning) (Phenyl trimethicone)
0.50
Permethyl 101A (Presperse, Inc.) (Isohexadecane)
1.00
Fixate Superhold Polymer (30% TS) (Lubrizol Advanced Materials) (Polyacrylate-2 crosspolymer)
10.00
Blue 1 (FD&C Blue No. 1 (0.5% Solution))
0.023
Timiron MP-149 Diamond Cluster (Merck KGaA/EMD Chemicals, Inc.) (Mica (and) titanium dioxide)
0.35
Timron Starlight Blue (Merck KGaA/EMD Chemicals, Inc.) (Mica (and) titanium dioxide)
0.15
Phenonip (Clariant International Ltd.) (Phenoxyethanol, methyl-, ethyl-, butyl-, propyl- (and) isobutylparaben)
0.70
Fragrance (Robertet) (Citric Apple #FR-646800)
0.25

Phase B
Deionized water
55.837

Phase C
Apifil (Gattefossu00e9 S.A.S.) (PEG-8 Beeswax)
2.00

Phase D
Pemulen TR-1 Polymer (Lubrizol Adv. Mat.) (Acrylates/C10-30 alkyl acrylate crosspolymer)
0.10

Phase E
Deionized water
3.00

Phase F
Triethanolamine (99%)
0.42

Phase G
Red 33 (D&C Red No. 33 (0.5% Solution))
0.01

Phase H
Triethanolamine (99%)
0.42

Procedure
Disperse PEG-90M into propylene glycol, and then add deionized water.  Mix until uniform. Set phase A aside. In a separate vessel, heat water (phase B) to 75-80°C. In a separate vessel, combine phase C ingredients and heat to 75-80°C. Add phase C to phase B with mixing.  Mix until uniform. Begin cooling batch to 55-60°C. Disperse Pemulen TR-1 Polymer into Permethyl 101A. When batch (phase B/C) has cooled to <60°C, add phase D to batch.  Mix until uniform. In a separate vessel, pre-mix ingredients. Add phase E to batch (phase B/C/D). Mix until uniform. Pre-neutralize batch with triethanolamine (99%). Mix until uniform. Continue cooling batch. Add phase A to batch (phase B/C/D/E). Mix until uniform. Continue cooling batch. When batch has cooled to 40°C, add phase G ingredients to batch in order. Mix well after each addition. Mix until uniform. Neutralize batch with triethanolamine (99%) to pH of 6.5 -7.0.  Mix until uniform.

Properties
Appearance: Violet fibery cream
pH: 6.5-7.0
Viscosity (mPa∙s)**: 17,000-22,000
Stability:  Passed 3 months @ 45°C,
              1 week @ 60°C, 5 cycles freeze/thaw
Mechanical Stiffness,
Force (Newtons):   5.41 N  Std. dev: +/- 2.02%

More Information
Lubrizol Advanced Materials Inc. (Noveon Consumer Specialties), 9911 Brecksville Road, Cleveland, OH 44141-3247,  Tel: 216-447-5000, 800-379-5389, Fax: 216-447-5250
 Website: www.personalcare.noveon.com
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