Formulary

Anti-Aging Day Care Emulsion SPF 24

October 1, 2009


Phase A
Parsol 1789 (DSM) (Butyl methoxydibenzoylmethane avobenzone; USAN)
3.00
Parsol SLX (DSM) (Polysilicone-15)
0.99
Parsol 340 (DSM) (Octocrylene; USAN)
2.70
dl-alpha -Tocopheryl acetate (DSM) (Tocopheryl acetate)
0.50
Amphisol K (DSM) (Potassium cetyl phosphate)
3.00
Estol 3650 (Croda) (Glyceryl myristate)
4.00
Lanette 16 (Cognis) (Cetyl alcohol)
2.00
Butylated hydroxytoluene (Merck) (BH)
0.05
Dow Corning 200/100 cs (Dow Corning)(Dimethicone)
2.00
Phenonip (Clariant) (Phenoxyethanol & methylparaben & ethylparaben & butylparaben & propylparaben & isobutylparaben)
0.80
Dub DIS (Stearinerie Dubois Fils) (Diisopropyl sebacate)
9.00
Cetiol B (Cognis) (Dibutyl adipate)
7.00
Antaron V-220 (ISP) (VP/Eicosene copolymer)
2.00
Keltrol (CP Kelco) (Xanthan Gum)
0.30
Dequest 2046 (Solutia) (Pentasodium ethylenediamine tetramethylenephosphonate)
0.50
D-Panthenol (DSM)(Panthenol)
1.00
Water dem.
46.78
Sodium hydroxide 10% sol.
3.00
Parsol HS (DSM) (Phenylbenzimidazole sulfonic acid (Ensulizole; USAN)
2.00
Folic acid (DSM)
0.03
Stay-C 50 (DSM) (Sodium ascorbyl phosphate)
0.30

Phase B
Glycerin (Cognis)
3.00

Phase C
Sodium hydroxide 10% sol.
0.65

Phase D
Water dem.
5.00

Procedure
Heat phase A to 85°C and stir until homogeneous. Heat phase B to 85°C and add to part A under agitation. Cool down the emulsion to 55°C and add phase C. When everything is homogenous add phase D pre-heated to 50°C. Be sure that the pH of Parsol HS solution is 7.0. If traces remain, add small quantities of the used neutralizing base until the particles are dissolved. Homogenize thoroughly and then with continued mixing cool down to ambient temperature. It is generally recommended to use vacuum while producing the emulsion.

Properties
pH—7.53; Viscosity—16800 cps (Brookfield, RV4,10 rpm); SPF in vivo—24.2; In vitro UVAPF (Colipa 2007); PA: UVAPF/SPF (50 labelled); ≥0.33; PFA—9.3 Critical Wavelength: 374 nm.

Notes
For U.S. (under new proposed final monograph), AP, EU, LA

More Information
DSM Nutritional Products, (973) 257-8501, Website:  www.nutraaccess.com
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