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January 2010 formulary:

DNA Protective Lotion with Preventhelia Broad Spectrum SPF 18.6 Sunscreen Cream Shampoo & Body Wash for Babies and Kids Omega-3 Hand Soap Moisturizing Hand Sanitizer with Vitamin E

Golden Bronze Cream-to-Powder Eyeshadow Economy Sulfate-Free Shampoo Lucidity Anhydrous Sunscreen Gel Hair Conditioning Mask

DNA Protective Lotion with Preventhelia

Phase Phase A

Deionized water

76.10

Ultrez 10 (Lubrizol) (Carbomer)

0.20

Hispagel 200 NS (Cognis Iberia/Centerchem)

3.00

Phase Phase B

Promulgen D (Lubrizol) (Cetearyl alcohol & ceteareth-20)

2.00

Cutina GMS-SE (Cognis) (Glyceryl stearate)

1.25

Myrj 59 (Croda) (PEG-100 stearate)

1.00

Tegosoft CT (Evonik) (Capric/caprylic triglyceride)

2.00

Stratagel 500 (Centerchem)

8.00

Phase Phase C

Sodium hydroxide (10% solution)

0.75

Phase Phase D

Diocide (Centerchem)

0.70

Preventhelia Solution (Lipotec/Centerchem)

5.00

Procedure::
Disperse carbomer in water, mix until uniform. Add remaining phase A ingredients, heat to 80°C. Heat phase B to 80°C. Add phase B to phase A under moderate mixing. Mix for 10 minutes. Begin cool down. At 50°C, add phase C (batch should be ~ pH 6.5) At 40°C, add phase D ingredients one at a time. Mix until uniform. Discontinue.

More info: :
Centerchem, Tel: 203-822-9800, Website: www.centerchem.com

Broad Spectrum SPF 18.6 Sunscreen Cream

Phase Phase A

Dow Corning 345 Fluid (Dow Corning) (Cyclopentasiloxane, cyclohexasiloxane)

4.00

Velvesil 125 (Momentive) (Cyclopentasiloxane,
C30-45 alkyl cetearyl dimethicone crosspolymer)

4.50

Phase Phase B

Water deionized

50.05

Versene NA (Dow Chemical) (Disodium EDTA)

0.10

Phase Phase C

Superol K, Glycerine 99.7% USP/FCC Kosher (P&G Chemicals) (glycerin)

4.00

Mikrokill COS (Arch Chemicals) (Phenoxyethanol, caprylyl glycol, chlorphenesin)

1.00

Phase Phase D

X-Tend 226 (ISP) (Phenethyl benzoate)

5.00

HallBrite HS USP (HallStar) (Homosalate [homosalate])

7.50

HallBrite OS USP (HallStar) (Ethylhexyl salicylate [octisalate])

5.00

SolaStay S1 (HallStar) (Ethylhexyl methoxycrylene)

6.00

Phase Phase E

Parsol 1789 (DSM Nutritional) (Butyl methoxydibenzoylmethane [avobenzone])

3.00

Phase Phase F

HallStar GMS SE/AS (HallStar) (Glyceryl stearate, PEG-100 stearate)

1.00

HallStar TA-1618 (HallStar) (Cetearyl alcohol)

0.35

Ganex V-220 (ISP) (VP/eicosene copolymer)

1.00

Emulsiphos (Symrise) (Potassium cetyl phosphate,
hydrogenated palm glycerides)

3.00

Phase Phase G

Simulgel 600 (Seppic) (Acrylamide/sodium acryloyldimethyltaurate copolymer, isohexadecane, polysorbate 80

2.50

Phase Phase H

MSS-500W (Kobo Products) (Silica)

2.00

Procedure::
In a suitably rated vessel, premix phase A until homogeneous and smooth, then set aside for later use. Meanwhile add phase B to main vessel, commence center-stir (prop) mixing, start heating to 85°C, and add premixed phase C. To a third vessel add phase D, start mixing, add phase E and, when dissolved, heat to 85°C, then add phase F in order. With both phases at 85°C and homogeneous, add oil phase DEF to water phase BC with stirring and stop heating. After mixing for 10 minutes, homogenize until batch reaches 55°C and then resume sweep mixing while cooling. At 50°C or lower add phase G and when smooth add phase A. When again smooth, add phase H, replace any water lost to evaporation, and mix until smooth. When at desired filling temperature, stop cooling and mixing, perform final quality assurance checks and package product.

Properties::
Appearance—Light yellow cream; pH—6.4; Viscosity (RV, T-D, 5, 20 & 100 rpm, cP)—92000, 28000 & 7320.

More info::
The HallStar Company, Tel: (877) 427-4255, (312) 385-4494; Website: www.hallstar.com

Shampoo & Body Wash for Babies and Kids

Phase Phase A

1. Deionized water

77.32

2. Texapon KD (54% TS) (Cognis) (Ammonium lauryl sulfate (and) ammonium laureth sulfate (and) lauryl
glucoside (and) cocamide DEA

15.00

3. Chemonic LI-7 Surfactant (Lubrizol) (100%TS) (PEG-7 Glycerol coconate)

1.00

4. Mackam 2C (38% active) (Rhodia) (Disodium cocoamphodiacetate)

1.00

5. Chembetaine C surfactant (Lubrizol) (Cocamidopropyl betaine)

2.00

Phase Phase B

6. Glucamate DOE-120 Thickener (Lubrizol) (PEG-120 methyl glucose dioleate)

1.50

Phase Phase C

7. Glucquat 125 humectant (25% active) (Lubrizol) (Lauryl methyl gluceth-10 hydroxypropyldimonium chloride)

1.50

8. Euxyl K 300 (Schülke & Mayr) (Phenoxyethanol, methyl-, butyl-, propyl- (and) isobutylparaben)

0.30

9. Special fragrance #MX039168 (Belmay)

0.30

10. Citric acid (50% solution)

0.08

Procedure::
Phase A. In a suitable vessel combine ingredients in order one at a time with mixing. Mix until uniform. Add Glucamate DOE-120 thickener to batch and heat to 70-75°C. Mix until uniform. Remove heat and allow batch to slowly cool to 45°C with gentle mixing. When batch has cooled to 45°C, add ingredients 7-9 to batch in order, mix well after each addition. Mix until uniform. Adjust pH to 5.8-6.2 with citric acid (50% solution). Mix until uniform.

Properties::
Appearance—Clear liquid; pH—5.8–6.2; Viscosity (mPa·s) (Brookfield DV-II+ PRO @ 20 rpm, 25°C, #4 spindle, measured after 24 hours)—4,000–6,000; Stability—Passed 3 months@45°C, 4 cycles freeze/thaw.

More info::
Lubrizol Advanced Materials (Noveon Consumer Specialties), Tel: (216) 447-5000, (800) 379-5389, Website: www.personalcare.noveon.com

Omega-3 Hand Soap

Phase Phase A

Natunola Omega-3 oil gel 318 (Natunola)

0.25

Aloe vera oil gel C1XW (Natunola)

0.25

PPG-5-ceteth-20 (Croda)

2.00

Phase Phase B

Water

q.s.

Sodium laureth sulfate (Lubrizol)

15.0

Sodium lauroyl sarcosinate (Stepan)

20.0

Cocamidopropyl betaine (Cognis)

5.0

Methylparaben

0.2

Phase Phase C

Geoguard 221 (Lonza)

0.2

Citric acid

0.2

Sodium chloride

1.2

Color

q.s.

Fragrance

q.s.

Procedure::
In a batch tank, mix phase A and heat to 75°C. In a separate tank, heat the first four ingredients of phase B to 55°C. Add methylparaben and raise bath to 70°C. Add phase A into phase B. Begin cooling to room temperature. Add Geogard 221 and citric acid at 50°C. Adjust viscosity by using sodium chloride. Add color and fragrance if desired.

More info::
Natunola Health Inc., Tel: (613) 774-9998, Website: www.natunola.com

Moisturizing Hand Sanitizer with Vitamin E

Deionized water

31.25 grams

Ethanol (Pharmco Ethanol) (Ethyl alcohol, 200 proof)

65.00 grams

Glycerin

2.00 grams

Vitamin E USP (Jeen Int’l) (DL-alpha tocopheryl acetate)

0.25 grams

Benecel E10M (Ashland)

1.50 grams

Procedure::
Add Benecel to ethanol under good agitation to make a slurry, mix for 10 minutes or until all Benecel is wetted-out. Add water to the above slurry while mixing, mix for 45 minutes or until solution is smooth and lump free. Adjust mixing speed so that solution “turns-over.” Add other formulation ingredients while mixing. Continue mixing for 10 minutes.

Properties::
Viscosity Brookfield, RVT, 50rpm (cps)—1,325; pH—7.2; Clarity, % T, 600nm—96%.

More info::
Ashland Aqualon Functional Ingredients, Tel: (302) 995-3000, Website: www.aqualon.com

Golden Bronze Cream-to-Powder Eyeshadow

Phase Phase A

Tegosoft OP (Evonik Goldschmidt) (Octylpalmitate)

16.0

Tegosoft CO (Evonik Goldschmidt) (Cetyl octanoate)

14.0

Carnauba Wax 2442L

4.7

Abil Wax 2434 (Evonik Goldschmidt) (Stearoxy dimethicone)

6.0

Antaron V-220 (PVP/Eicosene copolymer)

1.0

Tegosoft SH (Evonik Goldschmidt) (Stearyl heptanoate)

16.0

Covabead LH85 (Polymethylmethacrylates)

6.0

Phase Phase B

Aerosil 200 (Evonik Degussa) (Silica)

3.0

Oxynex K liquid (PEG8 Tocopherol, ascorbyl palmitate, ascorbic acid, citric acid)

0.1

Preservative

q.s.

Phase Phase C

Talc Covasil 4.05 (Talc and dimethicone and trimethylsiloxysilicate)

6.0

Pemulen TR-2 (Acylates/C10-30 acyl acrylate crosspolymer)

2.0

Tegolon 12-10 (Evonik Goldschmidt) (Nylon-12)

2.0

Dryflo Pure (Aluminum starch octenylsuccinate)

6.0

Pigments (Mica/iron oxides/titanium dioxide/mica)

15.2

Timiron Supersheen MP-1001 (Mica, titanium dioxide)

2.0

Procedure::
Melt phase A at 85-87°C. Once phase A is completely melted add phase B and homogenize for 15 minutes. Pour or scoop into packaging while still hot. Smooth out tops with spatula when solidified. Pigment Blends—Gold: 50% Sunprizma Super Gold; 50% Sunpearl Gold. Dark Purple: 20% SunPrizma Concord Crush; 42% SunPrizma Cherry Marmalade; 22%; Spectraflex Focus Violet; 16% Sunprizma Sapphire Night.

More info::
Evonik Industries, Tel: 800 AEROSIL, (973) 541-8514, Website: www.aerosil.com

Economy Sulfate-Free Shampoo

Alpha-Step PC-48 (Stepan)

13.50

Amphosol CDB Special (Stepan)

10.00

Sodium chloride

1.50

Kathon CG (Rohm and Haas) (Methylychloroisothiazolinone and methylisothiazolinone)

0.05

Citric acid (25%)

q.s.

Fragrance and color

q.s.

Water

q.s. to 100.00

Procedure::
Add water to a container and turn on the agitator. Add surfactants and mix until homogeneous. Add sodium chloride to adjust viscosity. Add fragrance and dye under mixing. Adjust pH with citric acid or sodium or sodium hydroxide to pH between 5.0-5.5.

Properties::
pH as is—5.0-5.5; Viscosity at 25°C—3,500-6,200 cps; Appearance at 25°C—clear viscous liquid; Storage stability 4 weeks at 25°C—stable; Storage stability at 4 weeks at 50°C—stable; Freeze/thaw 3 cycles—requires gentle mixing after freezing.

More info::
Stepan Company, Tel: (847) 446-7500; Website: www.stepan.com

Lucidity Anhydrous Sunscreen Gel

Phase Phase A

Dow Corning EL-8050 ID Silicone Organic Elastomer Blend (Isododecane (and) bis-isobutyl PPG-20 crosspolymer)

67.45

Univul MC 80 (BASF) (Ethylhexyl methoxycinnamate)

7.50

Escalol 587 (ISP) (Octisalate)

5.00

Crodamol GTCC (Croda) (Caprylic/capric triglyceride)

8.00

Cetiol OE (Cognis) (Dicaprylyl ether)

12.00

Dow Corning VM-2270 Aerogel Fine Particles (Silica silylate)

0.05

Procedure::
Combine all ingredients except silica silylate in a mixing vessel. Mix at 700 rpm with marine propeller until homogeneous (at least 15 min). Increase mixing speed to 1000 rpm. Add silica silylate very slowly while continuing to mix until uniform.

More info::
Dow Corning Corporation, Tel: (989) 496-6000, Website: www.dowcorning.com/content/personal/

Hair Conditioning Mask

Phase Phase A

Cetearyl alcohol

4.00

Polawax GP-200 (Croda)

1.50

Methylparaben

0.10

Propylparaben

0.10

Phase Phase B

Deionized water

80.30

Celquat L-200 polymer (AzkoNobel) (Polyquaternium-4)

0.30

Structure Zea starch (Akzo Nobel) (Hydroxypropyl starch phosphate)

2.00

Varisoft BT 85 (Evonik) (Behentrimonium chloride)

2.00

Phase Phase C

Dow Corning 1501 Fluid (Dow Corning)(Cyclomethicone (and) dimethiconol)

2.00

Phase Phase D

Dow Corning 949 cationic emulsion (Dow Corning) (Amodimethicone (and) cetrimonium chloride
(and) trideceth-12)

2.00

Hydrovance moisturizing agent (AkzoNobel)
(Hydroxyethyl urea)

5.00

Triethyl citrate (Leimeng (China))

0.20

Triethanolamine (20%)

q.s. to pH 6.50

Glydant Plus Liquid (Lonza) (DMDM hydantoin (and) iodopropynyl butylcarbamate)

0.50

Procedure::
Combine all ingredients in phase A and heat to 80°C. For phase B, disperse the Structure Zea starch and Celquat L-200 polymer into water, add the Varisoft BT 85 with mixing, and heat to 80°C. Keep mixing until all the ingredients are well dispersed. While maintaining the 80°C temperature, add phase B to phase A with good agitation. Add phase C into phase AB at 70~75°C and then homogenize the batch for at least 10 minutes. Slowly keep mixing at 500 rpm and cool to 40°C. For phase D, premix the triethyl citrate into the Hydrovance moisturizing agent until dissolved. Add all the ingredients of phase D to phase ABC. Continue mixing the batch and cool to room temperature.

Properties::
pH—6.25-6.75 Viscosity—14,000-18,000 cps (Brookfield RVDV-II+, RV 6#, 10 rpm, 25°C).

More info::
AkzoNobel Surface Chemistry, Tel: (888) 331-6212, Website: www.akzonobel.com/PersonalCare