Oil-Free Creamy Face Wash

Released by AkzoNobel Surface Chemistry, Personal Care Applications

July 1, 2012

Phase A
Deionized water
Pricerine 9088 (Croda, Inc.) (Glycerin)
Dissolvine NA2-S chelate (AkzoNobel Func. Chem.) (Disodium EDTA)
Microcare CAG (Thor) (Caprylyl glycol)
Euxyl PE 9010 (Schu00fclke & Mayr) (Phenoxyethanol (and) ethylhexylglycerin)
Structure CEL 500 HM rheology modifier (AkzoNobel) (C12-16 alkyl PEG-2 hydroxypropyl hydroxyethyl ethylcellulose)
Prifrac 2962 (Croda) (Palmitic acid)
Pristerene 9559 (Croda) (Stearic acid)
Kessco PEG 6000 DS (Stepan) (PEG-150 distearate)
Protachem GC-7 (Protameen Chemicals Inc) (PEG-7 glyceryl cocoate)
Mackanate LO (Rhodia) (Disodium lauryl sulfosuccinate)
Amphosol 2C (38% Active) (Stepan) (Disodium cocoamphodiacetate)
Jarcol I-20 (Jarchem Industries) (Octyldodecanol)

Phase B
Prifrac 2942 (Croda) (Myristic acid)

Phase C
Potassium hydroxide 45% (Sigma-Aldrich)

Phase D

In ESCO 1L kettle, add all ingredients to kettle except Structure Cel 500 HM rheology modifier and begin mixing with sweep mixer and homogenizer speed set at 20. Begin heating to 80-85°C with water bath attachment to jacketed kettle ports. Sprinkle in Structure Cel 500 HM rheology modifier slowly and mix until fully dispersed. Once phase A reaches 80-85°C, add each phase B ingredients to the main kettle one at a time, mixing between additions until dispersed/dissolved. Hold batch temperature at 80-85°C. Once all phase B ingredients are added and fully incorporated into the batch, add Phase C ingredients to the main kettle. Homogenize with sweep mixing for 10 minutes at speed 30-40. Hold batch temperature at 80-85°C, then begin cooling batch down to 45°C after 10 minutes. Once batch reaches 45°C, add phase D and homogenize with sweep mixing at speed 30-40 until fully incorporated into formula. Mix only with sweep mixer at speed 10 and begin to pull vacuum at 4-6 psi (be careful not to suck formula through vacuum hose). Cool batch down to 25°C.

Appearanceu2014opaque cream; pHu20148.40 - 8.90 pH meter; Viscosityu2014200,000 -400,000, cps Brookfield RVT, Spindle F, Speed 10, 1 minute, 25°C; Packaging plastic heat seal top tube with wide orifice or a glass jar with cap.

More Information
AkzoNobel Surface Chemistry Global Personal Care
Phone: 888 331-6212
Fax: 908-707-3664
Email: personalcare.usa@akzonobel.comu00a0

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