Formulary

Color Protection Shampoo

Released by Ashland 04.02.18

Phase A
Deionized water	ad 100%
Dissolvine GL 38 (Akzo Nobel) (Tetrasodiumglutamate diacetate)	0.10
Timiron MP1001 (Merck)(Mica, titanium dioxide)	0.10
ChromoHance 113 polymer (Ashland) (Polyquaternium 113)	2.50
Cocamidopropyl betaine (30%) (Cocamidopropyl betaine)	6.67
Emal 228D (28%) (Kao) (Sodium laureth sulfate)	21.43
Phase B
Deionized water	20.00
Ashland 980 Carbomer (Ashland) (Carbomer)	0.40
Phase C
Optiphen 200 preservative (Ashland) (Phenoxyethanol and caprylyl glycol)	0.80
Nutritic karate (Robertet) (Parfum)	0.50
ClearHance C conditioning polymer (Ashland) (Cassia hydroxypropyltrimonium chloride)	0.20
Phase D
Ceraphyl 60 ester (Ashland)(Quaternium-22)	0.50
Belsil ADM 8301E (Wacker)(Amodimethicone/morpholinomethyl silsesquioxane,trideceth-5, glycerin)	1.50
Xiameter MEM 1788 (Xiameter) (Dimethiconol (and) TEA-dodecylbenzenesulfonate)	2.50
Phase E
Sodium hydroxide 33% (Sodium hydroxide)	0.30
Sodium chloride	1.00
Procedure
Phase A: Add the first 5 ingredients in the right order and wait after the addition of the cocamidopropyl betaine till the polymer is completely hydrated before continuing with the SLES (white haziness occur). Add the first portion of SLES, wait 5 minutes and add the second portion of SLES. Phase B: Dissolve the Carbomer in water until lump free and add to Phase A. Phase C: pre-disperse the Clearhance C in the perfume and Optiphen 200 and add to the mixer Phase D: Add the ingredients in order with good stirring. Phase E: Adjust the pH with Sodium Hydroxide 33% and Sodium Chloride to the desired pH and Viscosity.
Properties
Appearance— Creamy viscous liquid; pH—5.5 – 6.5; Viscosity (D0)—6,000 – 9,000 mPa.s Brookfield LVT Spindle #3, 12 RPM, 1 min @ 25°C; Stability—Pass 12 weeks @45°C. This formula has passed 3 M stability test at 45°C and 28-day double challenge efficacy test. However, the preservative system has not been optimized to its lowest effective level.
More Information
Ashland Tel.: 877-546-2782 Website: Ashland.com/personalcare