03.01.09
Phase A | |
Deionized water | 6.00 |
Propylene glycol | 8.00 |
Polyox WSR-301 (Dow/Amerchol) (PEG-90M) | 0.24 |
Cremophor A 25 (BASF Corp.) (Ceteareth-25) | 5.00 |
Schercemol PDD Ester (Lubrizol Adv. Mat.) (Diisostearoyl polyglyceryl-3 dimer dilinoleate) | 2.00 |
Petrolato Ambar 158 (Drogueria Cosmopolitan) (Petrolatum) | 4.00 |
Dow Corning 556 Cosmetic Grade Fluid (Dow Corning) (Phenyl trimethicone) | 0.50 |
Permethyl 101A (Presperse, Inc.) (Isohexadecane) | 1.00 |
Fixate Superhold Polymer (30% TS) (Lubrizol Advanced Materials) (Polyacrylate-2 crosspolymer) | 10.00 |
Blue 1 (FD&C Blue No. 1 (0.5% Solution)) | 0.023 |
Timiron MP-149 Diamond Cluster (Merck KGaA/EMD Chemicals, Inc.) (Mica (and) titanium dioxide) | 0.35 |
Timron Starlight Blue (Merck KGaA/EMD Chemicals, Inc.) (Mica (and) titanium dioxide) | 0.15 |
Phenonip (Clariant International Ltd.) (Phenoxyethanol, methyl-, ethyl-, butyl-, propyl- (and) isobutylparaben) | 0.70 |
Fragrance (Robertet) (Citric Apple #FR-646800) | 0.25 |
Phase B | |
Deionized water | 55.837 |
Phase C | |
Apifil (Gattefossu00e9 S.A.S.) (PEG-8 Beeswax) | 2.00 |
Phase D | |
Pemulen TR-1 Polymer (Lubrizol Adv. Mat.) (Acrylates/C10-30 alkyl acrylate crosspolymer) | 0.10 |
Phase E | |
Deionized water | 3.00 |
Phase F | |
Triethanolamine (99%) | 0.42 |
Phase G | |
Red 33 (D&C Red No. 33 (0.5% Solution)) | 0.01 |
Phase H | |
Triethanolamine (99%) | 0.42 |
Procedure | |
Disperse PEG-90M into propylene glycol, and then add deionized water. Mix until uniform. Set phase A aside. In a separate vessel, heat water (phase B) to 75-80°C. In a separate vessel, combine phase C ingredients and heat to 75-80°C. Add phase C to phase B with mixing. Mix until uniform. Begin cooling batch to 55-60°C. Disperse Pemulen TR-1 Polymer into Permethyl 101A. When batch (phase B/C) has cooled to <60°C, add phase D to batch. Mix until uniform. In a separate vessel, pre-mix ingredients. Add phase E to batch (phase B/C/D). Mix until uniform. Pre-neutralize batch with triethanolamine (99%). Mix until uniform. Continue cooling batch. Add phase A to batch (phase B/C/D/E). Mix until uniform. Continue cooling batch. When batch has cooled to 40°C, add phase G ingredients to batch in order. Mix well after each addition. Mix until uniform. Neutralize batch with triethanolamine (99%) to pH of 6.5 -7.0. Mix until uniform. | |
Properties | |
Appearance: Violet fibery cream pH: 6.5-7.0 Viscosity (mPa∙s)**: 17,000-22,000 Stability: Passed 3 months @ 45°C, 1 week @ 60°C, 5 cycles freeze/thaw Mechanical Stiffness, Force (Newtons): 5.41 N Std. dev: +/- 2.02% | |
More Information | |
Lubrizol Advanced Materials Inc. (Noveon Consumer Specialties), 9911 Brecksville Road, Cleveland, OH 44141-3247, Tel: 216-447-5000, 800-379-5389, Fax: 216-447-5250 Website: www.personalcare.noveon.com |